10L – IIII Short Path Distillation

Application Scope:

Liquid mixture.

Each component with different boiling points that vary greatly.

Advantages of Distillation:

Compared to other separation methods, such as extraction, filtration and crystallization, it has the advantage that no other solvents than system components are required, thus ensuring that no new impurities are introduced.

Product Name: Short Path Distillation and Extraction Equipment

Product Brand: Henan Lanphan

Product Specifications: 2/5/10/20L

Product Material: High Borosilicate Glass

Category:

  What is Short Path Distillation

As a type of thermodynamic separation technology, the equipment can evaporate components with low boiling points by utilizing that the boiling point of each component in the mixed liquid or liquid-solid mixture is different, and then condense the material to separate the whole components. It is the combination of evaporation and condensation unit operations as well as a kind of liquid-liquid separation technology.

  Why Use Short Path Distillation

The short path distillation is a technique that removes solvents from mixtures through evaporation, which is mainly used for liquid-liquid separation. As one of the most high-efficiency distillation techniques in people’s using, it can solve the problems that conventional distillation technology can’t.

As well, there are other possible reasons why the short path distillation is so widely used. Firstly, it requires a smaller working space compared to most conventional distillation techniques, which is much easier to use. And the desired purity level can also be reached. Secondly, it has a relatively low distillation temperature. Compared to the simple distillation, the materials can be separated even though there is a small temperature difference. Thirdly, the short path distillation is a physical process, which can well protect separated substances from being polluted and damaged. Furthermore, the less material will be lost because the liquid only need travel a short distance in the short path distillation. It efficiently reduces material waste. Therefore, the short path distillation has become more and more well-received.

  how does short path distillation work

  1. Molecules diffuse from the liquid phase to the evaporation surface:

The beginning of the short path distillation’s working is from evaporation flask. Sample will be placed in the evaporation flask and be heated by the heating mantle. The temperature that heating mantle provides can be adjusted according to the boiling points of different solvents.

  2. Free evaporation of molecules on the liquid surface:

The evaporation speed of solvents can be changed by the heating temperature. Besides, the stability of sample solvents is also an important factor influencing the evaporation speed.

  3. Molecules fly from the evaporation to the condensation surface:

The extracted gas-phase solvents will be transferred along a short distance, and be condensed along this distance. During this process, gas-phase solvents will be cooled down by the condensing part and turned into liquid-phase solvents.

  4. Solvents will be collected in the receiving flask:

After gas-phase solvents being turned into liquid-phase solvents, it will be transferred into receiving flask and be collected efficiently. Collecting extracted solvents in the receiving flask is very convenient for users to get.

In the whole working process of short path distillation, there are always vacuum pump providing vacuum and condensing part turning gas-phase solvents into liquid-phase solvents.

  Equipment List:

Accessories List of 10L Short Path Distillation Equipment
No. Name of Parts Specification Quantity Unit Notes
1 Double-Mouth Reaction Flask 10L 1 piece
2 Distiller custom-made model 1 piece
3 Connecting Valve 1 piece
4 Round-Bottom Flask 3000ml 1 piece
5 Cold Trap 2 pieces
6 Cold Trap Cover 2 pieces
7 Receiving Flask 500ml 2 pieces
8 Connecting Pipe 1 piece
9 Temperature Casing 2 pieces
10 Temperature Measuring Glass Tube 1 1 piece long pattern
11 Temperature Measuring Glass Tube 2 1 piece short pattern
12 Hollow Plug 2 pieces
13 Funnel 110mm 1 piece
14 Temperature Gauge 1 piece
15 Vacuum Gauge 1 piece
16 GL14 Cover 3 pieces
17 Stainless Steel Flask Clamp 1 1 piece
18 Stainless Steel Flask Clamp 2 10 pieces
19 Lifting Platform 1 piece stainless steel
20 Iron Support 1 1 piece
21 Iron Support 2 1 piece
22 Cross Bar 2 pieces stainless steel
23 Cross Clamp 1 8 pieces
24 Cross Clamp 2 5 pieces
25 Three-Jaw Clamp 3 pieces
26 Experimental Chain Clamp 2 pieces
27 Adapter 1 piece PTFE
28 Heating Mantle 220V/110V 1 piece

  Accessories Diagram:

Three-Jaw Clamp
Three-Jaw Clamp
PTFE Vacuum Gauge
PTFE Vacuum Gauge
KF25 Pagoda Head
KF25 Pagoda Head
KF25 PTFE Head
KF25 PTFE Head
KF25 Clamp
KF25 Clamp
Iron Support
Iron Support
Cold Trap Cover
Cold Trap Cover
500ml Receiving Flask
500ml Receiving Flask
10L Reaction Flask
10L Reaction Flask
3L Receiving Flask
3L Receiving Flask
Stainless Steel Equal-Diameter Tee
Stainless Steel Equal-Diameter Tee
Temperature Measuring Glass Tube
Temperature Measuring Glass Tube
Stainless Steel Clamp
Stainless Steel Clamp
PTFE Vacuum Gauge
PTFE Vacuum Gauge
Electronic Temperature Gauge
Electronic Temperature Gauge
Cross Clamp
Cross Clamp

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

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